Combustible Dust Testing

Laboratory testing to quantify dust explosion and reactivity hazards

Safety Data Sheets

Develop critical safety data for inclusion in SDS documents

Gas and Vapor

Laboratory testing to quantify explosion hazards for vapor and gas mixtures

UN-DOT
Classification of hazardous materials subject to shipping and storage regulations
Hydrogen
Testing and consulting on the explosion risks associated with devices and processes which use or produce hydrogen
Safety Data Sheets

Develop critical safety data for inclusion in SDS documents

Thermal Stability

Safe storage or processing requires an understanding of the possible hazards associated with sensitivity to variations in temperature

Adiabatic Calorimetry
Data demonstrate the consequences of process upsets, such as failed equipment or improper procedures, and guide mitigation strategies including Emergency Relief System (ERS) design
Reaction Calorimetry
Data yield heat and gas removal requirements to control the desired process chemistry
Battery Safety

Testing to support safe design of batteries and electrical power backup facilities particularly to satisfy UL9540a ed.4

Safety Data Sheets

Develop critical safety data for inclusion in SDS documents

Cable Testing
Evaluate electrical cables to demonstrate reliability and identify defects or degradation
Equipment Qualification (EQ)
Testing and analysis to ensure that critical equipment will operate under adverse environmental conditions
Water Hammer
Analysis and testing to identify and prevent unwanted hydraulic pressure transients in process piping
Acoustic Vibration
Identify and eliminate potential sources of unwanted vibration in piping and structural systems
Gas & Air Intrusion
Analysis and testing to identify and prevent intrusion of gas or air in piping systems
ISO/IEC 17025:2017

Fauske & Associates fulfills the requirements of ISO/IEC 17025:2017 in the field of Testing

ISO 9001:2015
Fauske & Associates fulfills the requirements of ISO 9001:2015
Dust Hazards Analysis
Evaluate your process to identify combustible dust hazards and perform dust explosion testing
On-Site Risk Management
On-site safety studies can help identify explosibility and chemical reaction hazards so that appropriate testing, simulations, or calculations are identified to support safe scale up
DIERS Methodology
Design emergency pressure relief systems to mitigate the consequences of unwanted chemical reactivity and account for two-phase flow using the right tools and methods
Deflagrations (Dust/Vapor/Gas)

Properly size pressure relief vents to protect your processes from dust, vapor, and gas explosions

Effluent Handling

Pressure relief sizing is just the first step and it is critical to safely handle the effluent discharge from an overpressure event

FATE™ & Facility Modeling

FATE (Facility Flow, Aerosol, Thermal, and Explosion) is a flexible, fast-running code developed and maintained by Fauske and Associates under an ASME NQA-1 compliant QA program.

Mechanical, Piping, and Electrical
Engineering and testing to support safe plant operations and develop solutions to problems in heat transfer, fluid, flow, and electric power systems
Hydrogen Safety
Testing and consulting on the explosion risks associated with devices and processes which use or produce hydrogen
Thermal Hydraulics
Testing and analysis to ensure that critical equipment will operate under adverse environmental conditions
Nuclear Safety
Our Nuclear Services Group is recognized for comprehensive evaluations to help commercial nuclear power plants operate efficiently and stay compliant
Radioactive Waste
Safety analysis to underpin decomissioning process at facilities which have produced or used radioactive nuclear materials
Adiabatic Safety Calorimeters (ARSST and VSP2)

Low thermal inertial adiabatic calorimeters specially designed to provide directly scalable data that are critical to safe process design

Other Lab Equipment and Parts for the DSC/ARC/ARSST/VSP2 Calorimeters

Products and equipment for the process safety or process development laboratory

FERST

Software for emergency relief system design to ensure safe processing of reactive chemicals, including consideration of two-phase flow and runaway chemical reactions

FATE

Facility modeling software mechanistically tracks transport of heat, gasses, vapors, and aerosols for safety analysis of multi-room facilities

Blog

Our highly experienced team keeps you up-to-date on the latest process safety developments.

Process Safety Newsletter

Stay informed with our quarterly Process Safety Newsletters sharing topical articles and practical advice.

Resources

With over 40 years of industry expertise, we have a wealth of process safety knowledge to share.

Recent Posts

Flow Regime Determination in Emergency Relief System Design - Blowdown Testing

Posted by Fauske & Associates on 10.07.20

By Benjamin Doup Ph.D., Senior Nuclear and Chemical Engineer, Fauske & Associates, LLC

Flow regime determination in emergency relief system (ERS) design is an important aspect of process hazard analysis because it can impact your required vent size and will impact the quantity and rate of liquid material that is vented. In the summer edition of Fauske & Associates, LLC's Process Safety Newsletter, we discussed the characteristics and showed the modeling of the churn-turbulent (or churn) and bubbly flow regimes in the article "Flow Regime Characterization in Emergency Relief System Design".

 

In the current issue, we provide practical guidance on how to determine the expected flow regime under emergency relief venting conditions.

The flow regime during venting can be determined by running a blowdown test in the Vent Sizing Package 2 (VSP2TM). The VSP2 blowdown test procedures, test interpretation, potential missteps, and benchmark test results that are applicable for vapor systems will be discussed.

VSP2 Blowdown Test Procedures

The suggested approach is to simulate the upset scenario in the VSP2 and then depressurize the test cell using a vent located on the lid of the test cell. Figure 1 shows a schematic of the VSP2 setup in blowdown configuration. This configuration is applicable for many materials and tests. However, depending on the specific design of the blowdown test the following modifications may be investigated:

• If your material is not hazardous you may be able to route the vent line to an open vessel filled with room temperature water. The water will act as a quenching fluid for the hot effluent from the test cell.

• Multiple or larger vents on the containment vessel may be necessary in order to depressurize the containment vessel at a similar rate to the depressurization of the test cell.

• If the material being tested has a high vapor pressure at room temperature, valves may need to be installed on the fill line and vent line inside the containment vessel to prevent mass loss after the blowdown is complete.

Process hazard analysis blowdown configuration
Figure 1 Schematic of the VSP2 setup in blowdown configuration

 

The general blowdown test procedures are:

  1. Use set temperature to determine properties that are required for all-vapor critical flow and bubble rise velocities
  2. Determine bubble rise velocity (u) for the material of interest and for both bubbly and churn flows using Equation 1
  3. Determine critical all-vapor mass flux at the set conditions using Equation 2
  4. Determine the superficial vapor velocity through the test cell (jg) at disengagement using Equation 3
  5. Target a jg/u between 0.8-4 by adjusting the vent diameter and/or all-vapor discharge coefficient (i.e., length of the vent line)
  6. Start the VSP2 blowdown test using a specific upset scenario procedures
  7. Begin blowdown of the test cell and containment vessel when the set temperature is reached by opening the valves on the test cell and containment vessel.
    1. a. It may be necessary to begin the containment blowdown before the test cell blowdown to avoid crushing the test cell.
  8. Close the valves when test cell pressure reaches ambient pressure, which often occurs within 8 seconds.

The bubble rise velocities are 

process hazard analysis bubble rise-velocities (1)

 

 

 

 where          C = bubble rise velocity coefficient, 1.18 for bubbly flow and 1.53 for churn flows,

 g = acceleration due to gravity, m/s2

 ρf = liquid density, kg/m3

ρg = vapor density, kg/m3

  σ = surface tension, N/m

The critical all-vapor mass flux at the set conditions can be estimated using

Gg =Process hazard analysis all vapor mass flux(2)


where           
Gg = critical all-vapor mass flux kg/m2/s

  k = isentropic coefficient,

Ps = set pressure, Pa

The vapor superficial velocity through the VSP2 test cell can be estimated using

jg  =   process hazard analysis vapor superficial velocity     (3)

where     Avent = effective flow area of the vent on the VSP2 test cell, in2

     Ax = cross sectional area of the VSP2 test cell, in2

The VSP2 Blowdown Test Interpretation

The interpretation of the VSP2 blowdown test is as important (if not more important) than the design and execution of the blowdown test and is necessary for determining the flow regime of your material. The main indicator is mass remaining in the test cell after the blowdown. The final mass is used to obtain an average void fraction. The final void fraction is then compared with the disengagement void fraction for the bubbly and churn flow regimes to obtain similarities. The disengagement void fractions for the bubbly and churn flow regimes are determined using Equation 4 [1].

jprocess hazard analysis void fractions

where  C0 = distribution coefficient, 1.01 or 1.2 for bubbly flow and 1.5 for churn flow

        Untitled-5-1 = vessel average void fraction, 

Additional items that will aid in the interpretation of the blowdown test are estimating the mass loss from the test cell assuming all vapor flow and simulating the depressurization of the test cell. The simulation of the depressurization of the test cell allows the time dependent temperature and pressure measurements to be used in the comparison of churn and bubbly flow regime comparison along with the mass remaining in the test cell.

Potential Missteps

The results of the blowdown testing may not always be extremely clear. When disengagement occurs while the flow is sub-critical, the vapor superficial velocity can be much lower than the vapor superficial velocity used in the test design.
This will affect the expected vessel average void fraction for complete disengagement. In this case simulating the VSP2 blowdown test may be necessary in order to provide the temperature and pressure comparison and aid in helping predict the superficial velocity when disengagement occurs. Crushing the test cell indicates that the size or number of valves used to depressurize the containment may be too small. In this case, the test may need to be repeated using a larger number or size of valves to depressurize the containment vessel. Alternatively a heavier walled test cell could also be used.

Benchmark Test


Benchmark tests have been performed using tap water and soapy water. Table 1 shows the initial conditions and the results of the benchmark tests. Figure 2 plots Equation 4 and the final void fractions of the benchmark test. Dynamic simulations were performed to aid in the interpretation of the blowdown tests. These tests show that tap water is predicted to behave as churn flow with a distribution coefficient of 1.5 and soapy water is expected to behave as a foamy or bubbly flow with a distribution coefficient equal to 1.01, which is consistent with the large scale test results [1].

One of the reasons that the average void fractions for the tap water tests, derived from the final mass of the VSP2 blowdown tests, are above the churn-turbulent predicted average void fraction is that disengagement occurs before the depressurization is over. This leads to all-vapor flow during a portion of the depressurization and additional mass loss from the test cell. Figure 3 shows the comparison between the depressurization transient and dynamic simulations for the tap water and soapy water blowdown tests with 1/8” diameter vent lines. The good agreement between the depressurization data and the dynamic simulations provide further evidence that the flow regime classification based on the blowdown tests is consistent with large scale data.

Process hazard analysis test conditions

process hazard analysis blowdown benchmark

process hazard analysis depressurization comparison

 

Emergency Relief System Design Using DIERS Technology

For more information regarding relief system design, process hazard analysis, and other process safety testing news, subscribe below!

Subscribe to Process Safety News

References
1. Fisher, H.G., Forrest, H.S., Grossel, S.S., Huff , J.E., Muller, A.R., Noronha, J.A., Shaw, D.A., and Tilley, B.J., Emergency
Relief System Design Using DIERS Technology, The Design Institute for Emergency Relief Systems (DIERS ) – Project Manual, 1992.

 

Topics: Reactive Chemicals

cta-bg.jpg

Is My Dust Combustible?

A Flowchart To Help You Decide
Download Now